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Beilstein J. Org. Chem. 2012, 8, 1528–1535, doi:10.3762/bjoc.8.173
Graphical Abstract
Scheme 1: Mechanism of free radical ring-opening polymerization of 2-VCPs (In: initiator) [29-31].
Scheme 2: Synthesis of diethyl 2-vinyl-1,1-cyclopropanedicarboxylate [33].
Scheme 3: Two-step synthesis of the macromonomer 5 (In: Initiator, TEA: triethylamine).
Figure 1: MALDI-TOF MS of amino-terminated poly(NiPAAm) 3.
Figure 2: Optical transmittance of aqueous solutions (c = 20 mg/mL) of 3, 6 und 8 during heating.
Figure 3: 2D ROESY NMR spectrum of a 5/Me2-β-CD deuterated water solution.
Figure 4: Temperature-dependent transparency measurements of aqueous solution of the supramolecular complex 7...
Scheme 4: Homo- and copolymerization of macromonomer 5.